Design, Synthesis, and Biological Evaluation of Chemically and Biologically Diverse Pyrroquinoline Pseudo Natural Products

Angew Chem Int Ed Engl. 2021 Feb 23;60(9):4648-4656. doi: 10.1002/anie.202013731. Epub 2021 Jan 12.

Abstract

Natural product (NP) structures are a rich source of inspiration for the discovery of new biologically relevant chemical matter. In natural product inspired pseudo-NPs, NP-derived fragments are combined de novo in unprecedented arrangements. Described here is the design and synthesis of a 155-member pyrroquinoline pseudo-NP collection in which fragments characteristic of the tetrahydroquinoline and pyrrolidine NP classes are combined with eight different connectivities and regioisomeric arrangements. Cheminformatic analysis and biological evaluation of the compound collection by means of phenotyping in the morphological "cell painting" assay followed by principal component analysis revealed that the pseudo-NP classes are chemically diverse and that bioactivity patterns differ markedly, and are dependent on connectivity and regioisomeric arrangement of the fragments.

Keywords: cell painting; cheminformatics; cycloaddition; heterocycles; natural products.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biological Products / chemical synthesis*
  • Biological Products / chemistry
  • Cycloaddition Reaction
  • Drug Design
  • Principal Component Analysis
  • Pyrrolidines / chemistry*
  • Quinolines / chemistry*
  • Stereoisomerism

Substances

  • Biological Products
  • Pyrrolidines
  • Quinolines
  • pyrrolidine