Novel Biobased Self-Healing Ionomers Derived from Itaconic Acid Derivates

Macromol Rapid Commun. 2021 Apr;42(8):e2000636. doi: 10.1002/marc.202000636. Epub 2020 Dec 28.

Abstract

This article presents novel biobased ionomers featuring self-healing abilities. These smart materials are synthesized from itaconic acid derivates. Large quantities of itaconic acid can be produced from diverse biomass like corn, rice, and others. This study presents a comprehensive investigation of their thermal and mechanical properties via differential scanning calorimetry (DSC), thermo gravimetric analysis (TGA), and FT-Raman and FT-IR measurements as well as dynamic mechanic analysis. Within all these measurements, different kinds of structure-property relationships could be derived from these measurements. For example, the proportion of ionic groups enormously influences the self-healing efficiency. The investigation of the self-healing abilities reveals healing efficiencies up to 99% in 2 h at 90 °C for the itaconic acid based ionomer with the lowest ionic content.

Keywords: biobased materials; ionomers; poly (itaconic acid esters); renewable polymers; self-healing materials; smart materials.

MeSH terms

  • Calorimetry, Differential Scanning
  • Spectroscopy, Fourier Transform Infrared
  • Succinates*
  • Thermogravimetry

Substances

  • Succinates
  • itaconic acid