Coumarins, dihydroisocoumarins, a dibenzo- α-pyrone, a meroterpenoid, and a merodrimane from Talaromyces amestolkiae

Tetrahedron Lett. 2021 May 25:72:153067. doi: 10.1016/j.tetlet.2021.153067. Epub 2021 Apr 9.

Abstract

Chemical investigation of an organic extract of a fungus isolated from submerged wood collected from fresh water (strain G173), identified as a Talaromyces amestolkiae (Eurotiales; Trichocomaceae), led to the isolation of three coumarins, three dihydroisocoumarins, a dibenzo-α-pyrone, a meroterpenoid, and a merodrimane. Three of the isolated compounds, namely 7-chloropestalasin A (3), 4-hydroxyaspergillumarin (6), and ent-thailandolide B (9) were new. The structures were elucidated using a combination of spectroscopic and spectrometric techniques. The absolute configurations of 2, 3, 5, and 6 were established via a modified Mosher's ester method, whereas for 9 a combination of TDDFT ECD and ORD calculations were employed. Compounds 1-9 were evaluated for antimicrobial activity against a group of bacteria and fungi.

Keywords: Coumarins; Dibenzo-α-pyrones; Dihydroisocoumarins; Freshwater Fungi; Merodrimanes; Meroterpenoids.