Scanning electron microscopy observation of dentin bond interfaces in different types of resin luting cements

Dent Mater J. 2024 Mar 29;43(2):179-190. doi: 10.4012/dmj.2023-219. Epub 2024 Jan 20.

Abstract

This study aimed to observe and compare the resin luting cement (RLC)/dentin interfaces of different types of RLC systems with scanning electron microscopy (SEM). This study evaluated six self-adhesive resin luting cement systems (SARLCs), four systems combining a SARLC with a tooth primer (SARLCPs), and six conventional resin luting cement systems (CVRLCs). Cured resin composite rods were bonded to bovine dentin using RLCs in different etching modes. The morphological features at the interfaces were observed using SEM. Although all RLCs in etch-&-rinse (ER) mode showed a clear hybrid layer, most SARLCs had a thinner and more porous hybrid layer than the SARLCPs and CVRLCs. All SARLCPs with primer and CVRLCs showed a thin high-density layer below the primer layer in both etching modes. CVRLCs and SARLCPs with primer treatment systems may be more versatile and reliable when compared to simplified RLC systems.

Keywords: Etching mode; Hybrid layer; Reaction layer; Resin cement–dentin interface; SEM observation.

MeSH terms

  • Animals
  • Cattle
  • Composite Resins / chemistry
  • Dental Bonding*
  • Dental Cements
  • Dentin
  • Dentin-Bonding Agents / chemistry
  • Materials Testing
  • Microscopy, Electron, Scanning
  • Resin Cements* / chemistry
  • Surface Properties

Substances

  • Resin Cements
  • Dental Cements
  • Dentin-Bonding Agents
  • Composite Resins