A number of natural fibers are being proposed for use in composite materials, especially those extracted from local plants, especially those able to grow spontaneously as they are cost-efficient and have unexplored potential. Sansevieria cylindrica, within the Asparagaceae (previously Agavacae) family, has recently been considered for application in polymer and rubber matrix composites. However, its characterization and even the sorting out of technical fiber from the stem remains scarce, with little available data, as is often the case when the fabrication of textiles is not involved. In this study, Sansevieria cylindrica fibers were separated down to the dimensions of a filament at an 8-15 micron diameter from the stem of the plant, then characterized physically and chemically, using Fourier transform infrared spectroscopy (FTIR), morphologically by scanning electron microscopy (SEM), as well as their thermal degradation, by thermogravimetric analysis (TGA). Their crystallinity surface roughness was measured by X-ray diffraction (XRD) and atomic force microscopy (AFM), respectively. The results indicate over 70% cellulose fibers content with a very high crystallinity (92%) and small crystallite size (1.45 nm), which suggests a low water absorption, with thermal degradation peaking at 294°C. Despite this, due to the significant porosity of the cellular structure, the density of 1.06 g cm-3 is quite low for a mainly cellulose fiber. Roughness measurements indicate that the porosities and foamy structure result in a highly negative skewness (-3.953), in the presence of deep valleys, which may contribute to an effective relation with a covering resin.
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