Purification of Recombinant N-terminal Histidine-Tagged Arabidopsis thaliana Phosphoglycolate Phosphatase 1, Glycolate Oxidase 1 and 2, and Hydroxypyruvate Reductase 1

Methods Mol Biol. 2024:2792:97-111. doi: 10.1007/978-1-0716-3802-6_8.

Abstract

To measure the kinetic properties of photorespiratory enzymes, it is necessary to work with purified proteins. Protocols to purify photorespiratory enzymes from leaves of various plant species require several time-consuming steps. It is now possible to produce large quantities of recombinant proteins in bacterial cells. They can be rapidly purified as histidine-tagged recombinant proteins by immobilized metal affinity chromatography using Ni2+-NTA-agarose. This chapter describes protocols to purify several Arabidopsis thaliana His-tagged recombinant photorespiratory enzymes (phosphoglycolate phosphatase, glycolate oxidase, and hydroxypyruvate reductase) from Escherichia coli cell cultures using two bacterial strain-plasmid systems: BL21(DE3)-pET and LMG194-pBAD.

Keywords: Escherichia coli; Glycolate oxidase; His-tagged recombinant protein; Hydroxypyruvate reductase; Immobilized metal affinity chromatography; Phosphoglycolate phosphatase; Photorespiration; Rapid one-step protein purification.

MeSH terms

  • Alcohol Oxidoreductases* / chemistry
  • Alcohol Oxidoreductases* / genetics
  • Alcohol Oxidoreductases* / isolation & purification
  • Alcohol Oxidoreductases* / metabolism
  • Arabidopsis / genetics
  • Arabidopsis Proteins* / chemistry
  • Arabidopsis Proteins* / genetics
  • Arabidopsis Proteins* / isolation & purification
  • Arabidopsis Proteins* / metabolism
  • Chromatography, Affinity / methods
  • Escherichia coli* / genetics
  • Escherichia coli* / metabolism
  • Histidine / genetics
  • Histidine / metabolism
  • Hydroxypyruvate Reductase* / chemistry
  • Hydroxypyruvate Reductase* / genetics
  • Hydroxypyruvate Reductase* / metabolism
  • Phosphoric Monoester Hydrolases* / chemistry
  • Phosphoric Monoester Hydrolases* / genetics
  • Phosphoric Monoester Hydrolases* / isolation & purification
  • Phosphoric Monoester Hydrolases* / metabolism
  • Recombinant Proteins* / genetics
  • Recombinant Proteins* / isolation & purification
  • Recombinant Proteins* / metabolism

Substances

  • Alcohol Oxidoreductases
  • Arabidopsis Proteins
  • glycollate oxidase
  • Histidine
  • Hydroxypyruvate Reductase
  • phosphoglycolate phosphatase
  • Phosphoric Monoester Hydrolases
  • Recombinant Proteins