Solvent-assisted mechanochemical crystallization of the metal-free perovskite solid solution (H2dabco, H2hmta)NH4(BF4)3

Chem Commun (Camb). 2024 Oct 17;60(84):12181-12184. doi: 10.1039/d4cc04010d.

Abstract

All-proportional solid solutions of the metal-free perovskite (H2dabco1-y, H2hmtay)(NH4)(BF4)3 ((d,h)-BF4) were crystallized via a mechanochemical method. Their molecular dynamics depend on the ratio y with a compositional boundary at y = 0.43, where H2dabco2+ was deduced to be at a dynamic disorder state, even below phase transition temperature to a plastic crystalline phase seen at y = 0.