Benzoxaborinine, New Chemotype for Carbonic Anhydrase Inhibition: Ex Novo Synthesis, Crystallography, In Silico Studies, and Anti-Melanoma Cell Line Activity

J Med Chem. 2024 Oct 24;67(20):18221-18234. doi: 10.1021/acs.jmedchem.4c01516. Epub 2024 Oct 8.

Abstract

The benzoxaborinine scaffold, a homologue of benzoxaborole with an additional carbon atom in the boracycle, shows significant potential in developing new therapeutic agents. This study reports the synthesis, inhibition assays against four human carbonic anhydrase (hCA, EC 4.2.1.1) isoforms, and anti-melanoma evaluation of 7-aryl(thio)ureido-substituted benzoxaborinines. Some derivatives, particularly compound 11, exhibited potent inhibitory activity (below 65 nM) against hCA IX and XII and stronger antiproliferative effects than SLC-0111 on human melanoma cells under hypoxia. Crystallographic studies of benzoxaborinine 3 adducts with hCA I and II demonstrated the binding mode of this chemotype, revealing that although both benzoxaborinine 3 and benzoxaborole 10 share a similar zinc-binding mode, the expanded ring in benzoxaborinine led to a different orientation within the active site. These findings suggest that benzoxaborinines hold promise for designing novel carbonic anhydrase inhibitors.

MeSH terms

  • Antineoplastic Agents* / chemical synthesis
  • Antineoplastic Agents* / chemistry
  • Antineoplastic Agents* / pharmacology
  • Borinic Acids / chemical synthesis
  • Borinic Acids / chemistry
  • Borinic Acids / pharmacology
  • Boron Compounds* / chemical synthesis
  • Boron Compounds* / chemistry
  • Boron Compounds* / pharmacology
  • Carbonic Anhydrase Inhibitors* / chemical synthesis
  • Carbonic Anhydrase Inhibitors* / chemistry
  • Carbonic Anhydrase Inhibitors* / pharmacology
  • Carbonic Anhydrases* / metabolism
  • Cell Line, Tumor
  • Cell Proliferation / drug effects
  • Crystallography, X-Ray
  • Drug Screening Assays, Antitumor
  • Humans
  • Melanoma / drug therapy
  • Melanoma / pathology
  • Models, Molecular
  • Structure-Activity Relationship

Substances

  • Antineoplastic Agents
  • Boron Compounds
  • Carbonic Anhydrase Inhibitors
  • Carbonic Anhydrases
  • Borinic Acids