Polyethylene glycol-phospholipid functionalized single-walled carbon nanotubes for enhanced siRNA systemic delivery

Sci Rep. 2024 Dec 3;14(1):30098. doi: 10.1038/s41598-024-80646-1.

Abstract

Small interfering RNAs (siRNA) technology has emerged as a promising therapeutic tool for human health conditions like cancer due to its ability to regulate gene silencing. Despite FDA-approved, their delivery remains localized and limiting their systemic use. This study used single-walled carbon nanotubes (SWNTs) functionalized with polyethylene glycolated (PEGylated) phospholipids (PL-PEG) derivatives for systemic siRNA delivery. We developed an siRNA systemic delivery vehicle (SWNT-siRNA) by conjugating SWNT functionalized with PL-PEG containing either amine (PA) or maleimide (MA). The functionalized SWNT with a lower molecular weight of PA produced the SWNT-siRNA conjugate system with the highest stability and high siRNA loading quantity. The system delivered siRNA to a panel of tumour cell lines of different organs (i.e. HeLa, H1299 and MCF-7) and a non-cancerous human embryonic kidney 293 cells (HEK293T) with high biocompatibility and low toxicity. The cellular uptake of SWNT-siRNA conjugates by epithelial cells was found to be energy dependent. Importantly, the presence of P-glycoprotein, a marker for drug resistance, did not inhibit SWNT-mediated siRNA delivery. Mouse xenograft model further confirmed the potential of SWNT-siRNA conjugates with a significant gene knock-down without signs of acute toxicity. These findings pave the way for potential gene therapy applications using SWNTs as delivery vehicles.

Keywords: Gene silencing; PEGylated phospholipid; Single-walled carbon nanotubes; siRNA delivery.

MeSH terms

  • Animals
  • Cell Line, Tumor
  • Gene Silencing
  • Gene Transfer Techniques
  • HEK293 Cells
  • HeLa Cells
  • Humans
  • MCF-7 Cells
  • Mice
  • Nanotubes, Carbon* / chemistry
  • Phospholipids* / chemistry
  • Polyethylene Glycols* / chemistry
  • RNA, Small Interfering* / administration & dosage
  • Xenograft Model Antitumor Assays

Substances

  • Nanotubes, Carbon
  • RNA, Small Interfering
  • Polyethylene Glycols
  • Phospholipids