Functional expression and site-directed mutagenesis of a synthetic gene for alpha-bungarotoxin

J Biol Chem. 1994 Apr 15;269(15):11178-85.

Abstract

In order to explore the structure-function relationships of the curare mimetic alpha-neurotoxins we have constructed and cloned a synthetic gene for Bungarus multicinctus alpha-bungarotoxin which is expressed in Escherichia coli. The recombinant alpha-bungarotoxin is expressed as a fusion protein with alpha-bungarotoxin linked to the COOH-terminal end of the T7 Gene 9-encoded coat protein. After treatment of the fusion protein with Factor Xa protease, a recombinant alpha-bungarotoxin is released that co-migrates with authentic alpha-bungarotoxin upon reverse-phase high performance liquid chromatography and ion-exchange chromatography. Final yields of active recombinant alpha-bungarotoxin were about 0.4 mg/liter of starting bacterial culture. The recombinant alpha-bungarotoxin contains 10 additional residues linked to the NH2-terminal Ile of the alpha-bungarotoxin sequence due apparently to the inaccessibility of the engineered cleavage site to Factor Xa. Nevertheless, the recombinant alpha-bungarotoxin is capable of binding to the nicotinic acetylcholine receptor with an apparent affinity that is only decreased approximately 1.7-fold from that of authentic alpha-bungarotoxin. Alanine substitution of a residue, Asp30, highly conserved among alpha-neurotoxins and previously suggested to play a key role in receptor recognition, resulted in a recombinant alpha-bungarotoxin whose receptor binding activity is indistinguishable from authentic alpha-bungarotoxin.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Alanine
  • Amino Acid Sequence
  • Animals
  • Aspartic Acid
  • Base Sequence
  • Bungarotoxins / biosynthesis*
  • Bungarotoxins / isolation & purification
  • Bungarotoxins / metabolism
  • Cell Membrane / metabolism
  • Chromatography, DEAE-Cellulose
  • Cloning, Molecular
  • Electric Organ / metabolism
  • Escherichia coli
  • Factor Xa / metabolism
  • Gene Expression*
  • Genes, Synthetic*
  • Models, Molecular
  • Molecular Sequence Data
  • Mutagenesis, Site-Directed
  • Oligodeoxyribonucleotides / chemical synthesis
  • Point Mutation
  • Protein Folding
  • Protein Structure, Secondary
  • Recombinant Fusion Proteins / biosynthesis
  • Recombinant Fusion Proteins / isolation & purification
  • Recombinant Proteins / biosynthesis
  • Recombinant Proteins / isolation & purification
  • Recombinant Proteins / metabolism
  • Snakes
  • Torpedo / metabolism

Substances

  • Bungarotoxins
  • Oligodeoxyribonucleotides
  • Recombinant Fusion Proteins
  • Recombinant Proteins
  • Aspartic Acid
  • Factor Xa
  • Alanine