Purification and molecular cloning of a novel acidic calmodulin binding protein from rat brain

J Biol Chem. 1993 Jun 25;268(18):13703-9.

Abstract

An acidic protein was identified among the insoluble proteins of a growth cone-enriched fraction, and this protein was purified from the Triton- and high NaCl-insoluble fraction of newborn rat brain using several column chromatographies after solubilization at an alkaline condition. The purified protein showed a Ca(2+)-dependent calmodulin binding activity. This protein showed an anomalous behavior in SDS-polyacrylamide gel electrophoresis as that observed in case of GAP-43 (neuromodulin, F1, pp46, p57, B-50) and MARCKS (p87, p80), namely shifts of apparent molecular weights under different acrylamide concentrations. Its physicochemical characteristics, such as heat stability, acidic isoelectric point, and solubility in a 2.5% perchloric acid solution, also resemble the properties of these proteins. cDNA cloning of this protein showed that the NH2-terminal 50-amino acid sequence was almost identical to CAP-23, a previously reported chicken protein of unknown function. Since the COOH-terminal half-regions of these proteins are less similar, the entire sequences of these proteins have 65% homology (52% identity), suggesting that these proteins belong to a family. Immunoblotting of several tissue extracts using a monoclonal antibody against this protein showed its specific expression in brain.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Animals
  • Base Sequence
  • Brain Chemistry*
  • Calmodulin-Binding Proteins / chemistry
  • Calmodulin-Binding Proteins / genetics
  • Calmodulin-Binding Proteins / isolation & purification*
  • Chromatography, Affinity
  • Chromatography, Gel
  • Cloning, Molecular
  • Connexins
  • Cytoskeletal Proteins / chemistry
  • DNA
  • Electrophoresis, Polyacrylamide Gel
  • Hydrogen-Ion Concentration
  • Intracellular Signaling Peptides and Proteins*
  • Membrane Proteins / chemistry
  • Molecular Sequence Data
  • Myristoylated Alanine-Rich C Kinase Substrate
  • Nerve Tissue Proteins / chemistry
  • Nerve Tissue Proteins / genetics
  • Nerve Tissue Proteins / isolation & purification*
  • Proteins / chemistry
  • Rats
  • Sequence Homology, Amino Acid

Substances

  • Calmodulin-Binding Proteins
  • Connexins
  • Cytoskeletal Proteins
  • Intracellular Signaling Peptides and Proteins
  • Marcks protein, rat
  • Membrane Proteins
  • Nerve Tissue Proteins
  • Proteins
  • Myristoylated Alanine-Rich C Kinase Substrate
  • Basp1 protein, rat
  • DNA

Associated data

  • GENBANK/D14441