Isolation of mitogenic glycophosphopeptides from cheese whey protein concentrate

Biosci Biotechnol Biochem. 1996 Mar;60(3):429-33. doi: 10.1271/bbb.60.429.

Abstract

We investigated the immunological function of cheese whey protein concentrate (CWPC), which is a by-product of cheese production, using mitogenic activity in murine splenocytes as an index. A fraction isolated by gel filtration and anion exchange chromatography of CWPC showed high mitogenic activity, comparable to the activity of lipopolysaccharide (LPS). The fraction was detected as a single band on SDS-PAGE. It contained calcium, inorganic phosphorus, and carbohydrate, indicating the active component to be a glycophosphopeptide (GPP). Since Pronase digestion of GPP did not reduce its mitogenic activity, carbohydrate rather than peptide may be important in the activity. When applied on an anti-beta-caseinophosphopeptide (beta-CPP) antibody affinity column, the GPP was separated into two components, one with affinity to beta-CPP and the other without such affinity. Both the components contained N-linked oligosaccharide chains and had the mitogenic activity. These results demonstrate that cheese whey contains a GPP having strong mitogenic activity.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adjuvants, Immunologic / isolation & purification
  • Adjuvants, Immunologic / pharmacology
  • Animals
  • Carbohydrates / analysis
  • Cheese / analysis*
  • Glycopeptides / immunology
  • Glycopeptides / isolation & purification*
  • Glycopeptides / pharmacology*
  • Lymphocyte Activation / drug effects
  • Lymphocyte Activation / immunology
  • Male
  • Mice
  • Mice, Inbred BALB C
  • Milk Proteins / chemistry*
  • Milk Proteins / immunology
  • Milk Proteins / pharmacology
  • Mitogens / isolation & purification*
  • Mitogens / pharmacology*
  • Phosphopeptides / immunology
  • Phosphopeptides / isolation & purification*
  • Phosphopeptides / pharmacology*
  • Spleen / cytology
  • Spleen / drug effects
  • Spleen / immunology
  • Whey Proteins

Substances

  • Adjuvants, Immunologic
  • Carbohydrates
  • Glycopeptides
  • Milk Proteins
  • Mitogens
  • Phosphopeptides
  • Whey Proteins