Projection structures of three photosynthetic complexes from Rhodobacter sphaeroides: LH2 at 6 A, LH1 and RC-LH1 at 25 A

J Mol Biol. 1998 Oct 2;282(4):833-45. doi: 10.1006/jmbi.1998.2050.

Abstract

Three photosynthetic complexes, light-harvesting complex 2 (LH2), light-harvesting complex 1 (LH1), and the reaction centre-light-harvesting complex 1 photounit (RC-LH1), were purified from a single species of a purple bacterium, Rhodobacter sphaeroides, and reconstituted into two-dimensional (2-D) crystals. Vesicular 2-D crystals of LH1 and RC-LH1 were imaged in negative stain and projection maps at 25 A resolution were produced. The rings formed by LH1 have approximately the same mean diameter as the LH1 rings from Rhodospirillum rubrum ( approximately 90 A) and therefore are likely to be composed of 15 to 17 alphabeta subunits. In the projection map calculated from the RC-LH1 2-D crystals, the reaction centre is represented by an additional density in the centre of the ring formed by the LH1 subunits. The marked improvement of shape and fine structure after a rotational pre-alignment of the RC-LH1 unit cells before averaging strongly suggests that the RC is not in a unique orientation within the LH1 rings. Tubular crystals of LH2 showed a high degree of order and allowed calculation of a projection map at 6 A resolution from glucose-embedded specimens. The projection structure shows a ring of nine alphabeta subunits. Variation of the alpha-helical projection densities suggests that the 9-fold symmetry axis is tilted with respect to the membrane normal.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacterial Proteins*
  • Cell Membrane / chemistry
  • Cell Membrane / metabolism
  • Crystallization
  • Glucose
  • Light-Harvesting Protein Complexes*
  • Microscopy, Electron
  • Phosphatidylcholines
  • Photosynthetic Reaction Center Complex Proteins / chemistry
  • Photosynthetic Reaction Center Complex Proteins / isolation & purification
  • Photosynthetic Reaction Center Complex Proteins / ultrastructure*
  • Protein Structure, Secondary
  • Rhodobacter sphaeroides / chemistry*
  • Solubility
  • Spectrum Analysis

Substances

  • Bacterial Proteins
  • Light-Harvesting Protein Complexes
  • Phosphatidylcholines
  • Photosynthetic Reaction Center Complex Proteins
  • light-harvesting complex 1, Rhodospirillum
  • 1,2-oleoylphosphatidylcholine
  • Glucose