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Sequential C-H Arylation and Enantioselective Hydrogenation Enables Ideal Asymmetric Entry to the Indenopiperidine Core of an 11β-HSD-1 Inhibitor.
Wei X, Qu B, Zeng X, Savoie J, Fandrick KR, Desrosiers JN, Tcyrulnikov S, Marsini MA, Buono FG, Li Z, Yang BS, Tang W, Haddad N, Gutierrez O, Wang J, Lee H, Ma S, Campbell S, Lorenz JC, Eckhardt M, Himmelsbach F, Peters S, Patel ND, Tan Z, Yee NK, Song JJ, Roschangar F, Kozlowski MC, Senanayake CH. Wei X, et al. Among authors: lee h. J Am Chem Soc. 2016 Nov 30;138(47):15473-15481. doi: 10.1021/jacs.6b09764. Epub 2016 Nov 17. J Am Chem Soc. 2016. PMID: 27794616 Free PMC article.
A superior method for the reduction of secondary phosphine oxides.
Busacca CA, Lorenz JC, Grinberg N, Haddad N, Hrapchak M, Latli B, Lee H, Sabila P, Saha A, Sarvestani M, Shen S, Varsolona R, Wei X, Senanayake CH. Busacca CA, et al. Among authors: lee h. Org Lett. 2005 Sep 15;7(19):4277-80. doi: 10.1021/ol0517832. Org Lett. 2005. PMID: 16146406
Asymmetric hydrogenation of unsaturated ureas with the BIPI ligands.
Busacca CA, Lorenz JC, Grinberg N, Haddad N, Lee H, Li Z, Liang M, Reeves D, Saha A, Varsolona R, Senanayake CH. Busacca CA, et al. Among authors: lee h. Org Lett. 2008 Jan 17;10(2):341-4. doi: 10.1021/ol7028542. Epub 2007 Dec 21. Org Lett. 2008. PMID: 18095698
Reduction of tertiary phosphine oxides with DIBAL-H.
Busacca CA, Raju R, Grinberg N, Haddad N, James-Jones P, Lee H, Lorenz JC, Saha A, Senanayake CH. Busacca CA, et al. Among authors: lee h. J Org Chem. 2008 Feb 15;73(4):1524-31. doi: 10.1021/jo7024064. Epub 2008 Jan 16. J Org Chem. 2008. PMID: 18197688
On the racemization of chiral imidazolines.
Busacca CA, Bartholomeyzik T, Cheekoori S, Grinberg N, Lee H, Ma S, Saha A, Shen S, Senanayake CH. Busacca CA, et al. Among authors: lee h. J Org Chem. 2008 Dec 19;73(24):9756-61. doi: 10.1021/jo8024384. J Org Chem. 2008. PMID: 19053584
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